Cr

Materials qualification of reactor structural materials is a critical step in rapid implementation of advanced nuclear reactor technologies, particularly to assess the corrosion performance in these designs. Accelerated qualification of reactor structural materials requires incorporating powerful computational toolsets, such as phase field modelling in the Multiphysics Object-Oriented Simulation Environment (MOOSE) framework, to predict the evolution of structural materials due to corrosion. Accordingly, computational toolsets will require experimental data generated at appropriate length scales to validate accuracy. Focused ion beam (FIB) provides a high degree of control over manipulation of materials for analytical purposes, including capturing data on the evolution in the microstructure and elemental composition of materials at the mesoscale, an appropriate length scale for phase field modelling of intergranular diffusion phenomena using the MOOSE framework. For instance, the FEI Helios G4 UX dual beam plasma FIB microscope at the Irradiated Materials Characterization Laboratory (IMCL) is capable of backscatter diffraction (EBSD) and energy-dispersive x-ray spectroscopy (EDS) documenting the evolution in the microstructure and elemental composition, respectively. The Helios can perform EDS and EBSD three-dimensionally (3D) using tomography, which is then combined using different software packages to visualize 3D volumes correlating elemental composition to microstructural data. The purpose of this investigation was to develop a streamlined characterization and data processing workflow for 3D tomography studies on the FEI Helios G4 plasma FIB. The investigation is segmented into three parts: 1) Optimizing the data collection workflow, 2) identifying appropriate data processing and visualization software (i.e. DREAM.3D, MIPAR, and VGStudioMax), and 3) establishing an infrastructure for public release. The optimization of the data collection workflow is in collaboration with members of the U220 department to setup formal training on the tomography operation of the G4, through ThermoFisher Scientific, and exploring DREAM.3D, MIPAR, and VGStudioMax data processing/visualization software packages. VGStudioMax currently demonstrates the most promise for future use. Optimization of the data collection and processing workflow is still ongoing. A collaboration with INL High Performance Computing (HPC) established an open-source license for expediting the public release of FIB tomography datasets through HPC. FIB tomography data generated by the G4 will provide comprehensive data for validating 3D phase field mesoscale modelling tools within the MOOSE framework for accelerated qualification of reactor structural materials.

Data and Resources

Datatype Name Last Modified
PNG
Cr EDS 3D.png

February 16, 2024, 18:08 (UTC)
Cr EDS.xdmf

February 16, 2024, 18:08 (UTC)
EBSD - SliceImage - 012_0_CrK.ipr

February 16, 2024, 18:08 (UTC)
EBSD - SliceImage - 001_0_CrK.dat

February 16, 2024, 18:08 (UTC)
EBSD - SliceImage - 012_0_CrK.dat

February 16, 2024, 18:08 (UTC)
EBSD - SliceImage - 001_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
PNG
EBSD - SliceImage - 013_Cr.png

February 16, 2024, 18:09 (UTC)
PNG
EBSD - SliceImage - 001_Cr.png

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 014_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 002_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 014_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 002_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
PNG
EBSD - SliceImage - 014_Cr.png

February 16, 2024, 18:09 (UTC)
PNG
EBSD - SliceImage - 002_Cr.png

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 015_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 003_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 015_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 003_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
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EBSD - SliceImage - 015_Cr.png

February 16, 2024, 18:09 (UTC)
PNG
EBSD - SliceImage - 003_Cr.png

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 016_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 004_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 016_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 004_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
PNG
EBSD - SliceImage - 016_Cr.png

February 16, 2024, 18:09 (UTC)
PNG
EBSD - SliceImage - 004_Cr.png

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 017_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 005_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 017_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 005_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
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EBSD - SliceImage - 017_Cr.png

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PNG
EBSD - SliceImage - 005_Cr.png

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EBSD - SliceImage - 018_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 006_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 018_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 006_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
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EBSD - SliceImage - 018_Cr.png

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EBSD - SliceImage - 006_Cr.png

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 019_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 007_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 019_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 007_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
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EBSD - SliceImage - 019_Cr.png

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EBSD - SliceImage - 007_Cr.png

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EBSD - SliceImage - 020_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 008_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 020_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 008_0_CrK.ipr

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EBSD - SliceImage - 020_Cr.png

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EBSD - SliceImage - 008_Cr.png

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EBSD - SliceImage - 021_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 009_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 021_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 009_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
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EBSD - SliceImage - 021_Cr.png

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EBSD - SliceImage - 009_Cr.png

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EBSD - SliceImage - 022_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 010_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 022_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 010_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
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EBSD - SliceImage - 022_Cr.png

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EBSD - SliceImage - 023_0_CrK.dat

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EBSD - SliceImage - 011_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 023_0_CrK.ipr

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EBSD - SliceImage - 012_Cr.png

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EBSD - SliceImage - 024_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 013_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 024_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 013_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 190_0_CrK.dat

February 16, 2024, 18:09 (UTC)
PNG
EBSD - SliceImage - 024_Cr.png

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 025_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 025_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
PNG
EBSD - SliceImage - 025_Cr.png

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 026_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 026_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
PNG
EBSD - SliceImage - 026_Cr.png

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 027_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 027_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
PNG
EBSD - SliceImage - 027_Cr.png

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 028_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 028_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
PNG
EBSD - SliceImage - 028_Cr.png

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 029_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 029_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
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EBSD - SliceImage - 029_Cr.png

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 030_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 030_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
PNG
EBSD - SliceImage - 030_Cr.png

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 031_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 031_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
PNG
EBSD - SliceImage - 031_Cr.png

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 032_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 032_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
PNG
EBSD - SliceImage - 032_Cr.png

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 033_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 033_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
PNG
EBSD - SliceImage - 033_Cr.png

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 034_0_CrK.dat

February 16, 2024, 18:09 (UTC)
EBSD - SliceImage - 034_0_CrK.ipr

February 16, 2024, 18:09 (UTC)
PNG
EBSD - SliceImage - 034_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 035_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 035_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
PNG
EBSD - SliceImage - 035_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 036_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 036_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
PNG
EBSD - SliceImage - 036_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 037_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 037_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
PNG
EBSD - SliceImage - 037_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 038_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 038_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
PNG
EBSD - SliceImage - 038_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 039_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 039_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
PNG
EBSD - SliceImage - 039_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 040_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 040_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
PNG
EBSD - SliceImage - 040_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 041_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 041_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
PNG
EBSD - SliceImage - 041_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 042_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 042_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
PNG
EBSD - SliceImage - 042_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 043_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 043_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
PNG
EBSD - SliceImage - 043_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 044_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 044_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
PNG
EBSD - SliceImage - 044_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 045_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 045_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
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EBSD - SliceImage - 045_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 046_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 046_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
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EBSD - SliceImage - 046_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 047_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 047_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
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EBSD - SliceImage - 047_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 048_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 048_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
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EBSD - SliceImage - 048_Cr.png

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EBSD - SliceImage - 049_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 049_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
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EBSD - SliceImage - 049_Cr.png

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EBSD - SliceImage - 050_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 050_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
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EBSD - SliceImage - 050_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 051_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 051_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
PNG
EBSD - SliceImage - 051_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 052_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 052_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
PNG
EBSD - SliceImage - 052_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 053_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 053_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
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EBSD - SliceImage - 053_Cr.png

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 054_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 054_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
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EBSD - SliceImage - 054_Cr.png

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EBSD - SliceImage - 055_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 055_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
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EBSD - SliceImage - 056_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 056_0_CrK.ipr

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EBSD - SliceImage - 056_Cr.png

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EBSD - SliceImage - 057_0_CrK.dat

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EBSD - SliceImage - 057_0_CrK.ipr

February 16, 2024, 18:10 (UTC)
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EBSD - SliceImage - 058_0_CrK.dat

February 16, 2024, 18:10 (UTC)
EBSD - SliceImage - 058_0_CrK.ipr

February 16, 2024, 18:11 (UTC)
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EBSD - SliceImage - 058_Cr.png

February 16, 2024, 18:11 (UTC)
EBSD - SliceImage - 059_0_CrK.dat

February 16, 2024, 18:11 (UTC)
EBSD - SliceImage - 059_0_CrK.ipr

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EBSD - SliceImage - 059_Cr.png

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EBSD - SliceImage - 060_0_CrK.dat

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EBSD - SliceImage - 061_0_CrK.dat

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EBSD - SliceImage - 062_0_CrK.dat

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EBSD - SliceImage - 164_0_CrK.dat

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EBSD - SliceImage - 165_0_CrK.dat

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EBSD - SliceImage - 178_0_CrK.dat

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EBSD - SliceImage - 166_0_CrK.dat

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EBSD - SliceImage - 179_0_CrK.dat

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EBSD - SliceImage - 167_0_CrK.dat

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EBSD - SliceImage - 180_0_CrK.dat

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EBSD - SliceImage - 168_0_CrK.dat

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EBSD - SliceImage - 181_0_CrK.dat

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EBSD - SliceImage - 169_0_CrK.dat

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EBSD - SliceImage - 181_0_CrK.ipr

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EBSD - SliceImage - 182_0_CrK.dat

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EBSD - SliceImage - 170_0_CrK.dat

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EBSD - SliceImage - 182_0_CrK.ipr

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EBSD - SliceImage - 183_0_CrK.dat

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EBSD - SliceImage - 171_0_CrK.dat

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EBSD - SliceImage - 183_0_CrK.ipr

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EBSD - SliceImage - 184_0_CrK.dat

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EBSD - SliceImage - 172_0_CrK.dat

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EBSD - SliceImage - 184_0_CrK.ipr

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EBSD - SliceImage - 185_0_CrK.dat

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EBSD - SliceImage - 173_0_CrK.dat

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EBSD - SliceImage - 185_0_CrK.ipr

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EBSD - SliceImage - 186_0_CrK.dat

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EBSD - SliceImage - 174_0_CrK.dat

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EBSD - SliceImage - 186_0_CrK.ipr

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EBSD - SliceImage - 187_0_CrK.dat

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EBSD - SliceImage - 175_0_CrK.dat

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EBSD - SliceImage - 188_0_CrK.dat

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EBSD - SliceImage - 176_0_CrK.dat

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EBSD - SliceImage - 189_0_CrK.dat

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EBSD - SliceImage - 177_0_CrK.dat

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EBSD - SliceImage - 189_0_CrK.ipr

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EBSD - SliceImage - 216_0_CrK.dat

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EBSD - SliceImage - 191_0_CrK.dat

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EBSD - SliceImage - 204_0_CrK.dat

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EBSD - SliceImage - 192_0_CrK.dat

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EBSD - SliceImage - 205_0_CrK.dat

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EBSD - SliceImage - 194_0_CrK.dat

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EBSD - SliceImage - 207_0_CrK.dat

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EBSD - SliceImage - 195_0_CrK.dat

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EBSD - SliceImage - 208_0_CrK.dat

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EBSD - SliceImage - 195_0_CrK.ipr

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EBSD - SliceImage - 196_0_CrK.dat

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EBSD - SliceImage - 209_0_CrK.dat

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EBSD - SliceImage - 196_0_CrK.ipr

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EBSD - SliceImage - 197_0_CrK.dat

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EBSD - SliceImage - 198_0_CrK.dat

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EBSD - SliceImage - 211_0_CrK.dat

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EBSD - SliceImage - 198_0_CrK.ipr

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EBSD - SliceImage - 199_0_CrK.dat

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EBSD - SliceImage - 212_0_CrK.dat

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EBSD - SliceImage - 217_0_CrK.dat

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EBSD - SliceImage - 230_0_CrK.dat

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EBSD - SliceImage - 218_0_CrK.dat

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EBSD - SliceImage - 231_0_CrK.dat

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EBSD - SliceImage - 218_0_CrK.ipr

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EBSD - SliceImage - 221_0_CrK.dat

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EDS.zip

June 7, 2024, 17:08 (UTC)
Cr EDS.dream3d

June 7, 2024, 18:13 (UTC)

Additional Info

Field Value
Author Trishelle Copeland-Johnson
Last Updated November 25, 2024, 20:12 (UTC)
Created February 16, 2024, 18:08 (UTC)
DOI Link https://doi.org/10.48806/2287679
Instrument FEI G4 Helios Hydra Plasma-FIB
Publication Copeland-Johnson TM, Murray DJ, Cao G and He L (2022) Assessing the interfacial corrosion mechanism of Inconel 617 in chloride molten salt corrosion using multi-modal advanced characterization techniques. Front. Nucl. Eng. 1:1049693. doi: 10.3389/fnuen.2022.1049693
Slice Offset 100 nm
Statement of Credit "Focused ion beam tomography of Alloy 617 corroded in molten chloride salt" by Trishelle Copeland-Johnson and Daniel J. J. Murray is licensed under CC BY 4.0 for distribution.