EDS

Particles comprised of a thermal neutron absorbing material (HfAl3) are dispersed in a metal matrix material with high thermal conductivity (aluminum) to conduct the heat generated by neutron capture away from the fuel and materials. This metal matrix composite is very promising for use as a conduction-cooled neutron absorber and has the potential to be useful as a shroud or heat sink for testing advanced fast reactor fuels and materials in an existing thermal reactor. To design and optimize the absorber block system for advanced reactor designs, fundamental understanding of the irradiation effect on material properties is necessary. This dataset contains TEM characterization results of neutron irradiated HfAl3-Al composite specimens. It is focused on the irradiation induced defects (dislocation lines and loops) characterization using the on-zone axis bright field STEM technique. This data was collected using a FEI Tecnai G2 F30 S/TEM at the Microscopy and Characterization Suite (MaCS), Center for Advanced Energy Studies (CAES).

Data and Resources

Datatype Name Last Modified
EDS02 linescan_BFSTEM 190kx region 4.emi

December 6, 2024, 19:18 (UTC)
EDS03 pointscan_BFSTEM 190kx region 3_4.ser

December 6, 2024, 19:18 (UTC)
EDS02 linescan_BFSTEM 190kx region 2_1.ser

December 6, 2024, 19:18 (UTC)
TIFF
EDS02 linescan_BFSTEM 190kx region 2.tif

December 6, 2024, 19:18 (UTC)
PNG
EDS02 linescan_BFSTEM 190kx region 2.png

December 6, 2024, 19:18 (UTC)
TIFF
EDS03 pointscan_BFSTEM 190kx region 3_2.tif

December 6, 2024, 19:18 (UTC)
PNG
EDS03 pointscan_BFSTEM 190kx region 3_2.png

December 6, 2024, 19:18 (UTC)
EDS02 linescan_BFSTEM 190kx region 4_1.ser

December 6, 2024, 19:18 (UTC)
TXT
EDS02_Al.txt

December 6, 2024, 19:18 (UTC)
EDS01 linescan_BFSTEM 190kx region 1_analysis.emi

December 6, 2024, 19:18 (UTC)
EDS03 pointscan_BFSTEM 190kx region 3_5.ser

December 6, 2024, 19:18 (UTC)
EDS01 linescan_BFSTEM 190kx region 1_1.ser

December 6, 2024, 19:18 (UTC)
EDS02 linescan_BFSTEM 190kx region 2.emi

December 6, 2024, 19:18 (UTC)
EDS03 pointscan_BFSTEM 190kx region 3_3.ser

December 6, 2024, 19:18 (UTC)
TXT
EDS02_O_region 4.txt

December 6, 2024, 19:18 (UTC)
EDS03 pointscan_BFSTEM 190kx region 3_2.ser

December 6, 2024, 19:18 (UTC)
EDS03 pointscan_BFSTEM 190kx region 3_1.ser

December 6, 2024, 19:18 (UTC)
TIFF
EDS01 linescan_BFSTEM 190kx region 1.tif

December 6, 2024, 19:18 (UTC)
PNG
EDS01 linescan_BFSTEM 190kx region 1.png

December 6, 2024, 19:18 (UTC)
EDS01 linescan_BFSTEM 190kx region 1.emi

December 6, 2024, 19:18 (UTC)
TXT
EDS01_Hf.txt

December 6, 2024, 19:18 (UTC)
TXT
EDS02_Hf_region 4.txt

December 6, 2024, 19:18 (UTC)
TXT
EDS01_Al.txt

December 6, 2024, 19:18 (UTC)
EDS03 pointscan_BFSTEM 190kx region 3.emi

December 6, 2024, 19:18 (UTC)
TIFF
EDS03 pointscan_BFSTEM 190kx region 3.tif

December 6, 2024, 19:18 (UTC)
PNG
EDS03 pointscan_BFSTEM 190kx region 3.png

December 6, 2024, 19:18 (UTC)
TXT
EDS02_Hf.txt

December 6, 2024, 19:18 (UTC)
TXT
EDS02_Al_region 4.txt

December 6, 2024, 19:18 (UTC)
PNG
EDS02 linescan_BFSTEM 190kx region 2_analysis.PNG

December 6, 2024, 19:18 (UTC)
TXT
EDS03 pointscan_BFSTEM 190kx region 3.txt

December 6, 2024, 19:18 (UTC)

Additional Info

Field Value
Author Donna Guillen, Yu Lu, Yaqiao Wu
Last Updated December 6, 2024, 19:18 (UTC)
Created December 6, 2024, 19:18 (UTC)
DOI Link https://doi.org/10.48806/2478162
Instrument FEI Tecnai G2 F30 STEM
Statement of Credit This work was performed by Battelle Energy Alliance, LLC under the DOE Idaho Operations Contract DE-AC07-05ID14517. Neutron irradiation in the ATR was conducted through DOE Office of Nuclear Energy, Nuclear Science User Facilities (NSUF) project BSU-15-8242. Post-irradiation examination was performed through NSUF Rapid Turnaround Experiment 21-4280.
parent_folder tem_characterization_of_neutron_irradiated_hfal3-al_composite_specimens_kgt_4105_after_nanomill
parent_title After Nanomill